Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Piperidine | HCID 8082 | — |
| Reactant | HCID 676224 | HCID 676224 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 19429657 | HCID 19429657 | — |
Reaction Steps
A mixture of 3.75 g 3,6-dichloro-2-methyl-benzo[b]-thiophene-1,1-dioxide and 35 ml piperidine is stirred for 4 hours at 80° C., water is subsequently added and it is extracted with ethyl acetate. The extract is concentrated by evaporation and it is ground with ethyl acetate. 1.6 g of the title compound (36% of the theoretical yield) of melting point 154°-156° C. is isolated.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US05547980 |
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| Source dataset | uspto-grants-1996_08 |
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| ORD ID | ord-e4c21e0384394d27814f7172c0de03ad |
|---|
| Source note | uspto-grants-1996_08 |
|---|
