HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → 5-chloro-N-[1-(4-chlorophenyl)-1-methylethyl]pentanamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | 5-Chlorovaleryl chloride | HCID 74089 | — |
| Reactant | 2-(4-Chlorophenyl)propan-2-amine hydrochloride | HCID 45158337 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | 5-chloro-N-[1-(4-chlorophenyl)-1-methylethyl]pentanamide | HCID 19429500 | — |
Reaction Steps
1-(4-Chlorophenyl)-1-methylethylamine hydrochloride (4.0 g) was reacted with 5-chloropentanoyl chloride (3.0 g) in dichloromethane (15 ml) containing triethylamine (8.1 ml) in a similar manner to Example 52b, to give 5-chloro-N-[1-(4-chlorophenyl)-1-methylethyl]pentanamide.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05547972 |
| Source dataset | uspto-grants-1996_08 |
| ORD ID | ord-27617f1506a84f9c8f93f0643724d8d4 |
| Source note | uspto-grants-1996_08 |