HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 19429426, compound → HCID 19429438, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 19429426 | HCID 19429426 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 19429438 | HCID 19429438 | — |
Reaction Steps
In a similar manner to Example 52d, a solution of N-[1-(4-chlorophenyl)-1-methylethyl]-5-(imidazol-1-yl)pentanamide (5.1 g) in THF (125 ml) was reduced with BH3 /THF (63.7 ml of a 1M solution) to give N-[1-(4-chlorophenyl)-1-methylethyl]-5-(imidazol-1-yl)pentylamine as an oil, b.p. 195° C. (0.05 mmHg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05547972 |
| Source dataset | uspto-grants-1996_08 |
| ORD ID | ord-60f8fe1c1f9940bdbc92377400312576 |
| Source note | uspto-grants-1996_08 |