Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | 8-Bromooctanoic acid | HCID 548275 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | 8-bromooctanoyl Chloride | HCID 11402228 | — |
Reaction Steps
A mixture of 8-bromooctanoic acid (26.4 g), thionyl chloride (40 ml) and acetonitrile (40 ml) was heated at 95° C. for 3 hours. The solvent was removed by distillation under vacuum and the residue purified by azeotropic distillation, using acetonitrile, to give 8-bromooctanoyl chloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US05547972 |
|---|
| Source dataset | uspto-grants-1996_08 |
|---|
| ORD ID | ord-433dc1d708cc440989b2780a342d26e0 |
|---|
| Source note | uspto-grants-1996_08 |
|---|
