HuagongsheHuagongshe Chemistry Print Report · For research reference only
Borane;tetrahydrofuran → HCID 19429375, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Borane;tetrahydrofuran | HCID 2723981 | — |
| Reactant | HCID 19429455 | HCID 19429455 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 19429375 | HCID 19429375 | — |
Reaction Steps
In a similar manner to Example 52d, a solution of N-[1-(4-chlorophenyl)-1-methylethyl]-8-(imidazol-1-yl)octanamide (5.9 g) in THF (130 ml) was reduced with BH3/THF (64.5 ml of a 1M solution) to give N-[1-(4-chlorophenyl)-1-methylethyl]-8-(imidazol-1-yl)octylamine, b.p. 210° C. (0.05 mmHg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05547972 |
| Source dataset | uspto-grants-1996_08 |
| ORD ID | ord-d1a7d4c714c94a28b646e1624ebf0e25 |
| Source note | uspto-grants-1996_08 |