HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 9863252, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 9863253 | HCID 9863253 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 9863252 | HCID 9863252 | — |
Reaction Steps
Ex 68b N-[1-(4-Chlorophenyl)-1-methylethyl]-3-(imidazol-1-yl)propylamine as an oil, b.p. 180° C. (0.05 mmHg) [Example 68(1)]. A sample of this oil was dissolved in ether and ethereal hydrogen chloride added. The solid obtained was collected by filtration, dried and recrystallised from propan-2-ol to give N-[1-(4-chlorophenyl)-1-methylethyl]-3-(imidazol-1-yl)propylamine dihydrochloride, m.p. 216°-218° C. [Example 68(2)].
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05547972 |
| Source dataset | uspto-grants-1996_08 |
| ORD ID | ord-c9ac588cd6d7412083b13749ff06b357 |
| Source note | uspto-grants-1996_08 |