Citric Acid → HCID 67588420, compound

Participants

Reaction Steps

N-[1-(4-Chlorophenyl)-1-methylethyl]-3-(imidazol-1-yl)propylamine (1.25 g) and citric acid (0.95 g) were dissolved in warm IMS (10 ml) and allowed to cool. After standing with occasional scratching a salt crystallised. The salt was collected by filtration, triturated with ethyl acetate/methanol (1:1) filtered and dried to give N-[1-(4-chlorophenyl)-1-methylethyl]-3-(imidazol-1-yl)propylamine citrate, m.p. 143°-145° C.

Provenance & Evidence