L-Tartaric acid → HCID 86749735, compound

Participants

Reaction Steps

N-[1-(4-Chlorophenyl)-1-methylethyl]-3-(imidazol-1-yl)propylamine (2.57 g) and L-(+)-tartaric acid (1.39 g) were dissolved in warm IMS (10 ml) and allowed to cool. On scratching a salt crystallised. The salt was collected by filtration and recrystallised from IMS to give N-[1-(4-chlorophenyl)-1-methylethyl]-3-(imidazol-1-yl)propylamine (+)tartrate dihydrate, m.p. 76°-78° C.

Provenance & Evidence