HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → N-[1-(4-chlorophenyl)ethyl]acrylamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | Acryloyl chloride | HCID 13140 | — |
| Reactant | 1-(4-Chlorophenyl)ethylamine | HCID 97803 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | N-[1-(4-chlorophenyl)ethyl]acrylamide | HCID 19429535 | — |
Reaction Steps
In a similar manner to Example 62a, a mixture of acryloyl chloride (58.2 g) was added to 1-(4-chlorophenyl)ethylamine (100 g) and triethylamine (65.2 g) in dichloromethane (400 ml) to give N-[1-(4-chlorophenyl)ethyl]acrylamide, m.p. 103°-104° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05547972 |
| Source dataset | uspto-grants-1996_08 |
| ORD ID | ord-ddfa316e95ac4ef8ac81c3f15efd662e |
| Source note | uspto-grants-1996_08 |