HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → HCID 19429720, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 19429704 | HCID 19429704 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 19429720 | HCID 19429720 | — |
Reaction Steps
990 mg (2.11 mmol) of this ester, in 25 ml of methanol, are treated with 2 g of sodium hydroxide. The reaction mixture is refluxed for 1 h and it is then treated as in Example 3. After recrystallization from absolute ethanol, 630 mg (66%) of the expected product are isolated, which product melts at 318°-320° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05547983 |
| Source dataset | uspto-grants-1996_08 |
| ORD ID | ord-d0651feda869468fb528e12b890b6b81 |
| Source note | uspto-grants-1996_08 |