HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → HCID 15290962, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | HCID 19428106 | HCID 19428106 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 15290962 | HCID 15290962 | — |
Reaction Steps
To 21.93 g of (±)-4-[3-(trifluoromethyl)benzoyl]-3,4-dihydro-2H-1,4-benzoxazine-3-ethanol dissolved in 280 ml of dichloromethane are added 18 ml (0.248 mol) of thionyl chloride and the mixture is stirred at room temperature for 6 h.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05550125 |
| Source dataset | uspto-grants-1996_08 |
| ORD ID | ord-5b065eff6d3a47ecb759eb0577d50d73 |
| Source note | uspto-grants-1996_08 |