HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → HCID 15290963, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | HCID 19428113 | HCID 19428113 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 15290963 | HCID 15290963 | — |
Reaction Steps
To 11.27 g (0.031 mol) of (±)-6-fluoro-4-[3-(trifluoromethyl)benzoyl]-3,4-dihydro-2H-1,4-benzoxazine-3-ethanol dissolved in 140 ml of dichloromethane are added 9 ml (0.124 mol) of thionyl chloride and the mixture is stirred at room temperature for 5 h.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05550125 |
| Source dataset | uspto-grants-1996_08 |
| ORD ID | ord-5f1f6ed2b7894a7aa707e30c3b4e5155 |
| Source note | uspto-grants-1996_08 |