HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → HCID 15290966, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | HCID 19428104 | HCID 19428104 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 15290966 | HCID 15290966 | — |
Reaction Steps
To 14.74 g (0.039 mol) of (±)-6-methoxy-4-[3-(trifluoromethyl)benzoyl]-3,4-dihydro-2H-1,4-benzoxazine-3-ethanol dissolved in 165 ml of dichloromethane are added 14 ml (0.19 mol) of thionyl chloride and the mixture is stirred at room temperature for 5 h.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05550125 |
| Source dataset | uspto-grants-1996_08 |
| ORD ID | ord-b678b4ea89bd4d4ab1866a18a8d8cad9 |
| Source note | uspto-grants-1996_08 |