HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-(2-Methoxyphenyl)piperazine → HCID 19428156, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-(2-Methoxyphenyl)piperazine | HCID 1346 | — |
| Reactant | HCID 19428145 | HCID 19428145 | — |
| Solvent | Chloroform ethanol | HCID 21889567 | — |
| Product | HCID 19428156 | HCID 19428156 | 54% |
Reaction Steps
Process A; starting materials: 6-ethoxy-3-[2-(methanesulphonyloxy)ethyl]-7-methoxy-4-methyl-2H-1-benzopyran-2-one (Example 29) and 1-(2-methoxyphenyl)piperazine; yield 54%; m.p. 143°-145° C. (from ethanol/chloroform).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05550129 |
| Source dataset | uspto-grants-1996_08 |
| ORD ID | ord-059fdfd5367d406392342d1869b10d37 |
| Source note | uspto-grants-1996_08 |