HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-(2-Ethoxyphenyl)piperazine → 3-{2-[4-(2-ethoxyphenyl)-1-piperazinyl]ethyl}-5,7-dimethoxy-4-methyl-2H-1-benzopyran-2-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-(2-Ethoxyphenyl)piperazine | HCID 83357 | — |
| Reactant | 3-(2-chloroethyl)-5,7-dimethoxy-4-methyl-2H-1-benzopyran-2-one | HCID 19428161 | — |
| Product | 3-{2-[4-(2-ethoxyphenyl)-1-piperazinyl]ethyl}-5,7-dimethoxy-4-methyl-2H-1-benzopyran-2-one | HCID 19428137 | 31% |
Reaction Steps
Process B: starting materials: 3-(2-chloroethyl)-5,7-dimethoxy-4-methyl-2H-1-benzopyran-2-one (Example 39) and 1-(2-ethoxyphenyl)piperazine; yield 31% of crude product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05550129 |
| Source dataset | uspto-grants-1996_08 |
| ORD ID | ord-2886c4eb72fa42749201d06ff52c2639 |
| Source note | uspto-grants-1996_08 |