HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 67690831, compound → HCID 9926785, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 67690831 | HCID 67690831 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 9926785 | HCID 9926785 | 30% |
Reaction Steps
Using the procedure of Example 2G with methanol as solvent at room temperature, the compound of step A (700 mg, 2.16 mmole) was reduced and the trans isomer 4-hydroxy-3-phenylmethyl-2H-1-benzopyran-7-propionic acid methyl ester saponified using the procedure of Example 2I to give the title compound (210 mg), 30% yield.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05550152 |
| Source dataset | uspto-grants-1996_08 |
| ORD ID | ord-056c1f2e592a41c29f5da65e4f2ac03b |
| Source note | uspto-grants-1996_08 |