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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1078726Generated: October 31, 2026

Hydrochloric Acid → HCID 70277877, compound

https://huagongshe.com/reaction/1078726

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHydrochloric AcidHCID 313—
ReactantMethanolHCID 887—
ReactantHCID 22865014HCID 22865014—
ProductHCID 70277877HCID 70277877—

Reaction Steps

(2S,4R)-N-tert-Butoxycarbonyl-4-tert-butyldimethylsiloxy-2-(3-tert-butyldimethylsiloxy-1-oxopropyl)pyrrolidine (4.87 g, 10.0 mmol) was dissolved in a 3.3N hydrogen chloride--methanol solution (16.5 ml). The solution was stirred at room temperature for 24 h, and then concentrated in vacuo to obtain the title compound (2.29 g).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05550121
Source datasetuspto-grants-1996_08
ORD IDord-68f60f7885c845d7b9a48238786ac111
Source noteuspto-grants-1996_08