HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 70277877, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Methanol | HCID 887 | — |
| Reactant | HCID 22865014 | HCID 22865014 | — |
| Product | HCID 70277877 | HCID 70277877 | — |
Reaction Steps
(2S,4R)-N-tert-Butoxycarbonyl-4-tert-butyldimethylsiloxy-2-(3-tert-butyldimethylsiloxy-1-oxopropyl)pyrrolidine (4.87 g, 10.0 mmol) was dissolved in a 3.3N hydrogen chloride--methanol solution (16.5 ml). The solution was stirred at room temperature for 24 h, and then concentrated in vacuo to obtain the title compound (2.29 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05550121 |
| Source dataset | uspto-grants-1996_08 |
| ORD ID | ord-68f60f7885c845d7b9a48238786ac111 |
| Source note | uspto-grants-1996_08 |