HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phosgene → Cyclopentyl chloroformate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phosgene | HCID 6371 | — |
| Reactant | Cyclopentanol | HCID 7298 | — |
| Solvent | Toluene | HCID 1140 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | Cyclopentyl chloroformate | HCID 2735892 | — |
Reaction Steps
A solution of 0.543 g of cyclopentyl alcohol in 15 ml of methylene chloride is added to a 0° C. solution of 1.0 ml of a 10% toluene solution of phosgene in toluene in 10 ml of methylene chloride. The reaction is allowed to warm to room temperature and is stirred for 3 hours. The reaction is concentrated at reduced pressure, diluted with 15 ml of toluene and reconcentrated to dryness to give the product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05550257 |
| Source dataset | uspto-grants-1996_08 |
| ORD ID | ord-c1d0e99bc6874afea7239da56800c2fa |
| Source note | uspto-grants-1996_08 |