HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 22134093, compound → HCID 19428705, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 22134093 | HCID 22134093 | — |
| Reactant | HCID 22146052 | HCID 22146052 | — |
| Reactant | Sodium t-butoxide | HCID 23676156 | — |
| Solvent | tert-Butyl methyl ether | HCID 15413 | — |
| Product | HCID 19428705 | HCID 19428705 | — |
Reaction Steps
25.6 g (83.6 mmol) of dioctyl phosphite are initially introduced into 100 ml of tert-butyl methyl ether, 0.4 g of sodium tert-butanolate are added, and 20.0 g (77.4 mmol) of dodecylthioacetone are subsequently introduced.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05550276 |
| Source dataset | uspto-grants-1996_08 |
| ORD ID | ord-64a8dc95002445a7a51ac310797f2802 |
| Source note | uspto-grants-1996_08 |