HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triphenylphosphine → [(3-Nitrophenyl)methyl](triphenyl)phosphanium bromide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triphenylphosphine | HCID 11776 | — |
| Reactant | Benzene, 1-(bromomethyl)-3-nitro- | HCID 77568 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | [(3-Nitrophenyl)methyl](triphenyl)phosphanium bromide | HCID 11454393 | — |
Reaction Steps
A solution of 3-nitrobenzylbromide (5 gm, 23 mmol) and triphenylphosphine (6.1 gm, 23 mmol) were stirred in toluene at 75° C. for 6 hr. After cooling to rt, the crystalline product was isolated by filtration. The product was washed with toluene and dried in vacuo.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05550233 |
| Source dataset | uspto-grants-1996_08 |
| ORD ID | ord-1fc262b1cf514be1a9c83a8d2c83c511 |
| Source note | uspto-grants-1996_08 |