反应详情

A solution of 3-nitrobenzylbromide (5 gm, 23 mmol) and triphenylphosphine (6.1 gm, 23 mmol) were stirred in toluene at 75° C. for 6 hr. After cooling to rt, the crystalline product was isolated by filtration. The product was washed with toluene and dried in vacuo.

1. customthe crystalline product was isolated by filtration
2. washThe product was washed with toluene
3. customdried in vacuo