Diisopropyl Ether → HCID 23367101, compound

HRID 1079466Notes

Reaction equation

HRID 1079466 reaction equation
[O:1]1[CH:5]=[CH:4][C:3]([O:6][CH2:7][C:8]([OH:10])=O)=[N:2]1.[N+]([O-])(O)=O.[O:15]([CH2:19][CH2:20][NH2:21])[N+:16]([O-:18])=[O:17].C(OC(C)C)(C)C>>[O:15]([CH2:19][CH2:20][NH:21][C:8](=[O:10])[CH2:7][O:6][C:3]1[CH:4]=[CH:5][O:1][N:2]=1)[N+:16]([O-:18])=[O:17]

Participants

4

Reactant 3

HCID 7914Diisopropyl EtherHCID 78397Ethanol, 2-amino-, 1-nitrate, nitrate (1:1)HCID 23367119HCID 23367119, compound

Product 1

HCID 23367101HCID 23367101, compoundYield 54.1%

Procedure

Following a similar treatment to that in Example 2 and using 286 mg of 3-isoxazolyloxyacetic acid and 338 mg of nitroxyethylamine nitrate, 250 mg of the title compound was obtained as colorless needles (solvent for recrystallization; diisopropyl ether).

Sources & evidence

ORD record
ord-d58e5983f8934f56ba1d7db19e45756c
Source dataset
uspto-grants-1996_12
Patent number
US05580893

Reaction notes

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