Diisopropyl Ether → HCID 23367109, compound

HRID 1079467Notes

Reaction equation

[O:1]1[CH:5]=[CH:4][C:3]([C:6]([OH:8])=O)=[CH:2]1.[N+]([O-])(O)=O.[O:13]([CH2:17][CH2:18][NH2:19])[N+:14]([O-:16])=[O:15].C(OC(C)C)(C)C>>[O:13]([CH2:17][CH2:18][NH:19][C:6]([C:3]1[CH:4]=[CH:5][O:1][CH:2]=1)=[O:8])[N+:14]([O-:16])=[O:15]

Participants

Reactant 3

HCID 7914Diisopropyl Ether

HCID 102683-Furoic acid

HCID 78397Ethanol, 2-amino-, 1-nitrate, nitrate (1:1)

Product 1

HCID 23367109HCID 23367109, compoundYield 42.2%

Procedure

Following a similar treatment to that in Example 2 and using 0.48 g of 3-furancarboxylic acid and 0.60 g of nitroxyethylamine nitrate, 0.30 g of the title compound was obtained as colorless plates (solvent for recrystallization; diisopropyl ether).

Sources & evidence

ORD record: ord-b5a44965439c4e3aab0f47c59d37e01c
Source dataset: uspto-grants-1996_12
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US05580893

Reaction notes

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