HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thiophene-3-carboxylic acid → HCID 23367108, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thiophene-3-carboxylic acid | HCID 6918 | — |
| Reactant | Diisopropyl Ether | HCID 7914 | — |
| Reactant | Ethanol, 2-amino-, 1-nitrate, nitrate (1:1) | HCID 78397 | — |
| Product | HCID 23367108 | HCID 23367108 | 35.2% |
Reaction Steps
Following a similar treatment to that in Example 2 and using 0.55 g of 3-thiophenecarboxylic acid and 0.60 g of nitroxyethylamine nitrate, 0.27 g of the title compound was obtained as colorless plates (solvent for recrystallization; diisopropyl ether).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05580893 |
| Source dataset | uspto-grants-1996_12 |
| ORD ID | ord-a77e1b4627254fa3be1df8e8098ae84a |
| Source note | uspto-grants-1996_12 |