Diisopropyl Ether → HCID 23367116, compound

HRID 1079470Notes

Reaction equation

HRID 1079470 reaction equation
[N+:1]([C:4]1[O:8][C:7]([C:9]([OH:11])=O)=[CH:6][CH:5]=1)([O-:3])=[O:2].[N+]([O-])(O)=O.[O:16]([CH2:20][CH2:21][NH2:22])[N+:17]([O-:19])=[O:18].C(OC(C)C)(C)C>>[O:16]([CH2:20][CH2:21][NH:22][C:9]([C:7]1[O:8][C:4]([N+:1]([O-:3])=[O:2])=[CH:5][CH:6]=1)=[O:11])[N+:17]([O-:19])=[O:18]

Participants

4

Reactant 3

HCID 7914Diisopropyl EtherHCID 125775-Nitro-2-Furoic AcidHCID 78397Ethanol, 2-amino-, 1-nitrate, nitrate (1:1)

Product 1

HCID 23367116HCID 23367116, compoundYield 28.7%

Procedure

Following a similar treatment to that in Example 2 and using 0.56 g of 5-nitro-2-furancarboxylic acid and 0.60 g of nitroxyethylamine nitrate, 0.25 g of the title compound was obtained as yellow plates (solvent for recrystallization; diisopropyl ether).

Sources & evidence

ORD record
ord-0d2c4d3b282b423faa44a525f4b83377
Source dataset
uspto-grants-1996_12
Patent number
US05580893

Reaction notes

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