2-Bromoethanol → HCID 23367168, compound

Participants

Reaction Steps

To the mixture of 4-methylthiazole (24 g) and dioxane (30 ml) was added 2-bromoethanol (40 g), and the resulting mixture was heated under reflux for 4 hours. To the reaction left standing at room temperature for about 0.5 hour was added acetone (100 ml) with stirring to give white to pale yellow solids, which were collected by filtration, washed with acetone and dried under reduced pressure.

Provenance & Evidence