HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol → HCID 67757980, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | 4-Methyl-5-(2-hydroxyethyl)thiazole | HCID 1136 | — |
| Reactant | N,N-Dimethylaminoethyl chloride hydrochloride | HCID 11636816 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | HCID 67757980 | HCID 67757980 | — |
Reaction Steps
To a mixture of 4-methyl-5-thiazole ethanol (16.0 g) and dimethylaminoethyl chloride hydrochloride (14.4 g) was added ethanol (10 ml. The mixture was heated under reflux for about 20 hours. Ethanol (10 ml) and acetone (100 ml) were added, and the mixture was stirred to give pale yellow powdery crystals, which were collected by filtration, washed with acetone containing a small amount of ethanol and dried under reduced pressure.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05580904 |
| Source dataset | uspto-grants-1996_12 |
| ORD ID | ord-8b4427ce23a844aaa4be4503851aa221 |
| Source note | uspto-grants-1996_12 |