HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 23365534, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | 6,7-Dimethoxy-1,2,3,4-tetrahydroisoquinoline hydrochloride | HCID 6456035 | — |
| Reactant | HCID 23365535 | HCID 23365535 | — |
| Solvent | Dimethylacetamide | HCID 31374 | — |
| Product | HCID 23365534 | HCID 23365534 | 38.4% |
Reaction Steps
Employing the procedure of Preparation B, 730 mg of 2,6-dichloro-7-(1-phenylethyl)purine, 573 mg of 1,2,3,4-tetrahydro-6,7-dimethoxyisoquinoline hydrochloride and 505 mg of triethylamine in 25 ml of dimethylacetamide gave 430 mg of the desired intermediate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05583137 |
| Source dataset | uspto-grants-1996_12 |
| ORD ID | ord-fe37add70d7e4222901a424290924231 |
| Source note | uspto-grants-1996_12 |