HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 23365519, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | 2,6-Dichloropurine | HCID 5324412 | — |
| Reactant | Isoquinoline, 1-((3,4-dimethoxyphenyl)methyl)-1,2,3,4-tetrahydro-6,7-dimethoxy-, hydrochloride (1:1) | HCID 16667431 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 23365519 | HCID 23365519 | 45.8% |
Reaction Steps
Using the procedure of Preparation D, 2.01 g of 2,6-dichloropurine, 3.76 g of 1,2,3,4-tetrahydro-1-(3,4-dimethoxybenzyl)-6,7-dimethoxyisoquinoline hydrochloride and 4 g of triethylamine in 20 ml of methylene chloride gave 2.31 g of the titled product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05583137 |
| Source dataset | uspto-grants-1996_12 |
| ORD ID | ord-f7e99b1b7d6b45849827a944a6f57594 |
| Source note | uspto-grants-1996_12 |