HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanol → HCID 252528, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | Hydroxy(4-isopropylphenyl)acetic acid | HCID 23423233 | — |
| Product | HCID 252528 | HCID 252528 | — |
Reaction Steps
To a solution of 4-isopropylmandelic acid (17 g) in methanol (150 ml) was added Dowex-50X-400® and the mixture was refluxed for 4 hours. After cooling it was filtered through Celite® and the filtrate was evaporated to give a syrupy residue of methyl 4-isopropylmandelate (18.9 g), which solidified upon storing at room temperature.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05583147 |
| Source dataset | uspto-grants-1996_12 |
| ORD ID | ord-a4414e79a9e04c73b0e36da095dee9bb |
| Source note | uspto-grants-1996_12 |