2-Methyl-3-butyn-2-ol → HCID 23366187, compound

HRID 1080888Notes

Reaction equation

HRID 1080888 reaction equation
[CH3:1][C:2]([OH:6])([CH3:5])[C:3]#[CH:4].[CH3:7][O:8][CH2:9][CH2:10]Br>>[CH3:7][O:8][CH2:9][CH2:10][O:6][C:2]([CH3:5])([CH3:1])[C:3]#[CH:4]

Participants

3

Reactant 2

HCID 82582-Methyl-3-butyn-2-olHCID 809722-Bromoethyl methyl ether

Product 1

HCID 23366187HCID 23366187, compoundYield 61.6%

Procedure

In accordance with the procedure of the step 1 of Example 10, and using 21.7 g of 3-methyl-1-butyn-3-ol and 39.4 g of 2-bromoethyl methyl ether, 22.6 g of 3-(2-methoxyethoxy)-3-methyl-1-butyne was obtained.

Sources & evidence

ORD record
ord-ae66bdb280bb426ebea4f0fcdd63209b
Source dataset
uspto-grants-1996_12
Patent number
US05583227

Reaction notes

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