Nitrogen → HCID 131719748, compound

HRID 1080931Notes

Reaction equation

HRID 1080931 reaction equation
N#N.[O:3]=[C:4]([CH:6]=[C:7]([CH3:9])[CH3:8])[CH3:5].C[CH:11]([CH2:13][C:14]([CH3:16])=[O:15])[CH3:12]>OS(O)(=O)=O>[OH:15][CH:14]([CH2:13][CH2:11][CH3:12])[CH2:16][C:4](=[O:3])[CH3:5].[CH3:5][C:4](=[O:3])[CH2:6][C:7]([CH3:9])([OH:15])[CH3:8]

Participants

5

Reactant 3

HCID 947NitrogenHCID 7909Methyl Isobutyl KetoneHCID 8858Mesityl oxide

Product 1

HCID 131719748HCID 131719748, compound

Reagents, catalysts & solvents 1

HCID 1118Sulfuric AcidCatalyst

Procedure

A 150 ml jacketed glass reactor was equipped with a thermocouple, magnetic stirrer, feed and sample ports, and an overhead condenser. The reactor was maintained under positive N2 atmosphere by connecting the condenser vent line to a N2 bubbler. Fifty ml (46.5 grams) of mesityl oxide heavy ends from the current MIBK process (the reaction medium for the dehydration reaction step), which contained the H2SO4 catalyst, was added to the reactor.

Workup

  1. customwas equipped with a thermocouple, magnetic stirrer, feed and sample ports, and an overhead condenser
  2. temperatureThe reactor was maintained under positive N2 atmosphere
  3. customfor the dehydration reaction step), which
  4. additionwas added to the reactor

Sources & evidence

ORD record
ord-efcc872c71c24d0eab10825628c0ffc6
Source dataset
uspto-grants-1996_12
Patent number
US05583263

Reaction notes

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