HuagongsheHuagongshe Chemistry Print Report · For research reference only
Imidazole → HCID 86750068, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Imidazole | HCID 795 | — |
| Reactant | Pyridine | HCID 1049 | — |
| Reactant | Chlorotrimethylsilane | HCID 6397 | — |
| Reactant | HCID 86750066 | HCID 86750066 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 86750068 | HCID 86750068 | 80.6% |
Reaction Steps
183 mg (0.52 mmol) of 51 is reacted with 171 mg (1.56 mmol) of trimethylchlorosilane, 140 mg (2.03 mmol) of imidazole and 0.21 ml of pyridine in 15 ml of diethyl ether analogously to 33., and 178 mg of the title compound is obtained as colorless oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05585368 |
| Source dataset | uspto-grants-1996_12 |
| ORD ID | ord-a8254b90657b4728812169f3ddcb42b5 |
| Source note | uspto-grants-1996_12 |