HuagongsheHuagongshe Chemistry Print Report · For research reference only
Tetrahydrofuran → HCID 86750071, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Tetrahydrofuran | HCID 8028 | — |
| Reactant | Diazomethane | HCID 9550 | — |
| Reactant | HCID 86750072 | HCID 86750072 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 86750071 | HCID 86750071 | — |
Reaction Steps
To a mixture of the compound obtained in Example 74 (50 mg) and THF (15 ml) was added a solution of diazomethane (excess) in ethyl ether. After the mixture was stirred for 30 minutes at room temperature, the solvent was evaporated to give the titled compound as colorless crystals (25 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05585385 |
| Source dataset | uspto-grants-1996_12 |
| ORD ID | ord-47c3b232cac14468a9735fdba68dd7df |
| Source note | uspto-grants-1996_12 |