HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Chloro-1,2-dinitrobenzene → HCID 22922483, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Chloro-1,2-dinitrobenzene | HCID 33097 | — |
| Reactant | tert-Octylamine | HCID 61017 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 22922483 | HCID 22922483 | 46.2% |
Reaction Steps
A mixture of 20 g of 4-chloro-1,2-dinitrobenzene and 30 g of tert-octylamine in 300 ml of 95° EtOH is refluxed for 16 hours. The solvent is evaporated off under vacuum to give 13 g of the expected product after crystallization from an iso ether/heptane mixture (40/60; v/v). M.p.=108° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05585394 |
| Source dataset | uspto-grants-1996_12 |
| ORD ID | ord-aa8b20be75e44803abd43febbb018557 |
| Source note | uspto-grants-1996_12 |