HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Chloro-1,2-dinitrobenzene → HCID 2916373, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Chloro-1,2-dinitrobenzene | HCID 33097 | — |
| Reactant | 2-Morpholinoethylamine | HCID 408285 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 2916373 | HCID 2916373 | 62.2% |
Reaction Steps
A mixture of 19.5 g of 4-chloro-1,2-dinitrobenzene and 35 g of 4-(2-aminoethyl)morpholine in 180 ml of EtOH is stirred for 20 hours at RT. The precipitate formed is filtered off and washed with iso ether to give 17.1 g of the expected product after crystallization twice in succession from isopropanol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05585394 |
| Source dataset | uspto-grants-1996_12 |
| ORD ID | ord-8dc179927a5c41398e904a454ab0b5e2 |
| Source note | uspto-grants-1996_12 |