HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 12318732, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | N-Aminomorpholine | HCID 20315 | — |
| Reactant | 4-Chloro-1,2-dinitrobenzene | HCID 33097 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 12318732 | HCID 12318732 | 52.8% |
Reaction Steps
A mixture of 45 g of 4-chloro-1,2-dinitrobenzene, 25 g of 4-aminomorpholine and 30 g of triethylamine in 250 ml of 96° EtOH is stirred for 48 hours at RT. The precipitate formed is filtered off and washed with iso ether to give 30.2 g of the expected product. M.p.=155° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05585394 |
| Source dataset | uspto-grants-1996_12 |
| ORD ID | ord-b7e1c26a2e2144048e08dae99710f779 |
| Source note | uspto-grants-1996_12 |