HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cyclopentylamine → HCID 22922572, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cyclopentylamine | HCID 2906 | — |
| Reactant | 4-Chloro-1,2-dinitrobenzene | HCID 33097 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 22922572 | HCID 22922572 | 58.9% |
Reaction Steps
A mixture of 20 g of 4-chloro-1,2-dinitrobenzene and 20 g of cyclopentylamine in 50 ml of 95° EtOH is stirred overnight at RT. The precipitate formed is filtered off and washed with 95° EtOH to give 14 g of the expected product. M.p.=75° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05585394 |
| Source dataset | uspto-grants-1996_12 |
| ORD ID | ord-f2d385f26c524438a93f2661c969b6e8 |
| Source note | uspto-grants-1996_12 |