Cyclopentylamine → HCID 22922572, compound

HRID 1081477Notes

Reaction equation

HRID 1081477 reaction equation
[Cl:1][C:2]1[CH:7]=[CH:6][C:5]([N+:8]([O-:10])=[O:9])=[C:4]([N+:11]([O-])=O)[CH:3]=1.[CH:14]1(N)[CH2:18][CH2:17][CH2:16][CH2:15]1>CCO>[Cl:1][C:2]1[CH:7]=[CH:6][C:5]([N+:8]([O-:10])=[O:9])=[C:4]([NH:11][CH:14]2[CH2:18][CH2:17][CH2:16][CH2:15]2)[CH:3]=1

Participants

4

Reactant 2

HCID 2906CyclopentylamineHCID 330974-Chloro-1,2-dinitrobenzene

Product 1

HCID 22922572HCID 22922572, compoundYield 58.9%

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

A mixture of 20 g of 4-chloro-1,2-dinitrobenzene and 20 g of cyclopentylamine in 50 ml of 95° EtOH is stirred overnight at RT. The precipitate formed is filtered off and washed with 95° EtOH to give 14 g of the expected product. M.p.=75° C.

Workup

  1. customThe precipitate formed
  2. filtrationis filtered off
  3. washwashed with 95° EtOH

Sources & evidence

ORD record
ord-f2d385f26c524438a93f2661c969b6e8
Source dataset
uspto-grants-1996_12
Patent number
US05585394

Reaction notes

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