HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Methoxy-4-nitrobenzenesulfonyl chloride → HCID 23364265, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Methoxy-4-nitrobenzenesulfonyl chloride | HCID 309458 | — |
| Reactant | HCID 54505929 | HCID 54505929 | — |
| Product | HCID 23364265 | HCID 23364265 | 65.1% |
Reaction Steps
This compound is prepared by the procedure described in EXAMPLE 37 step A) starting from 1 g of 5- ethoxy-1,3-dihydro-3-(pyrid-2-yl)-2H-benzimidazol-2-one and 1.2 g of 2-methoxy-4-nitrobenzenesulfonyl chloride. 1.2 g of the expected product are obtained after crystallization from iso ether. M.p.=175° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05585394 |
| Source dataset | uspto-grants-1996_12 |
| ORD ID | ord-5afa97fde1ab4f49a413e80c6d0035ef |
| Source note | uspto-grants-1996_12 |