HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → HCID 23363018, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 23363016 | HCID 23363016 | — |
| Reactant | HCID 178527775 | HCID 178527775 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 23363018 | HCID 23363018 | 62% |
Reaction Steps
2-Chloromethyl-3-methyl-4-(3-thienylmethylthio)pyridine hydrochloride, 2-mercapto-1H-benzimidazole and sodium hydroxide are reacted in ethanol at 25° C. for 20 h. After crystallization from toluene/methanol, the title compound is isolated. Yield: 62%, m.p. 161°-164° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05587389 |
| Source dataset | uspto-grants-1996_12 |
| ORD ID | ord-7634a6b2616f41a6b59981db3b1ebeb6 |
| Source note | uspto-grants-1996_12 |