HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → HCID 23363024, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 23363017 | HCID 23363017 | — |
| Reactant | HCID 178527775 | HCID 178527775 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 23363024 | HCID 23363024 | 56% |
Reaction Steps
2-Chloromethyl-3-methoxy-4-(2-thienylmethylthio)pyridine hydrochloride, 2-mercapto-1H-benzimidazole and sodium hydroxide are reacted in ethanol at 25° C. for 20 h. After crystallization from toluene/methanol, the title compound is isolated. Yield: 56%, m.p. 124°-127° C. 8. 2-{[[4-(2-Thienylmethylthio)-2,pyridinyl]methyl]thio}-1H-benzimidazole
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05587389 |
| Source dataset | uspto-grants-1996_12 |
| ORD ID | ord-07d74879ea694231bb08df86b7550fad |
| Source note | uspto-grants-1996_12 |