HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → HCID 178488133, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | 2-Chloromethyl-3-methyl-4-[2-(4-methyl-5-thiazolyl)ethylthio]pyridine hydrochloride | HCID 22117306 | — |
| Reactant | HCID 178488140 | HCID 178488140 | — |
| Product | HCID 178488133 | HCID 178488133 | — |
Reaction Steps
Following the procedure described in Example 1, the reaction of 5-methoxy-2-mercapto-1H-benzimidazole with 2-chloromethyl-3-methyl-4-[2-(4-methyl-5-thiazolyl)ethylthio]pyridine hydrochloride and aqueous sodium hydroxide solution gives the title compound as a yellow oil, from which a hydrochloride salt of the title compound is obtained as a colorless powder of m.p. 165° C (decomp.) by following the procedure described in Example 4.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05587389 |
| Source dataset | uspto-grants-1996_12 |
| ORD ID | ord-190f2e7e02504de8a5d1ed18c0edcf62 |
| Source note | uspto-grants-1996_12 |