Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Salicyl Alcohol | HCID 5146 | — |
| Reactant | 1H-1,2,4-Triazole | HCID 9257 | — |
| Product | HCID 3849418 | HCID 3849418 | 76% |
Reaction Steps
The mixture of 2-hydroxymethylphenol (25.3 g) and 1H-1,2,4-triazole (15.5 g) was agitated at about 160° C. for 1 hour. After left to stand for cooling, the mixture was solidified into crystal, which was then recrystallized from ethanol and collected to give the title compound (27 g; 76 %).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US05587392 |
|---|
| Source dataset | uspto-grants-1996_12 |
|---|
| ORD ID | ord-bf3853308ec64551a810bae3e216525d |
|---|
| Source note | uspto-grants-1996_12 |
|---|
