HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,5,8,11,14,17,20-Heptaoxadocosan-22-amine → N-[3,6,9,12,15,18,21-heptaoxadocos-1-y1]-2,3,4,5-tetraiodopyrrol-1-acetamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,5,8,11,14,17,20-Heptaoxadocosan-22-amine | HCID 18764651 | — |
| Reactant | 2,3,4,5-Tetraiodopyrrol-1-acetic acid ethyl ester | HCID 53944792 | — |
| Product | N-[3,6,9,12,15,18,21-heptaoxadocos-1-y1]-2,3,4,5-tetraiodopyrrol-1-acetamide | HCID 23363352 | 114.2% |
Reaction Steps
According to the procedure described in Ex. 2, 2.3 g of 2,3,4,5-tetraiodopyrrol-1-acetic acid ethyl ester (prepared according to the procedure described in Ex. 1) (0.00457 mol) and 23.27 g of compound B, 3,6,9,12,15,18,21-heptaoxadocosylamine, (0.0685 mol) are reacted. 3.82 g of N-[3,6,9,12,15,18,21-heptaoxadocos-1-y1]-2,3,4,5-tetraiodopyrrol-1-acetamide (0.0040 mol) are obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05587487 |
| Source dataset | uspto-grants-1996_12 |
| ORD ID | ord-c4f9e4cc5bd54f3da58656d69a4609a1 |
| Source note | uspto-grants-1996_12 |