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HRID1081969

反应详情

EQUATION

反应方程式

HRID 1081969 的结构方程式

REACTANTS

反应物

3
结构：C#C
HCID6326

Ethyne

C2H2

结构：[K+].[OH-]
HCID14797

Potassium hydroxide

HKO

结构：C[Si](C)(C)CCCO
HCID76213

3-(Trimethylsilyl)-1-propanol

C6H16OSi

PRODUCTS

生成物

1
结构：C=COCCC[Si](C)(C)C
HCID23363376

未命名化合物

收率 96%

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CS(C)=O
溶剂HCID679

Dimethyl sulfoxide

C2H6OS

PROCEDURE

实验过程

In a similar manner to Example 1, 25 g (0.19 mol) of 3-(trimethylsilyl)propanol, 2.5 g of KOH and 25 g of DMSO were reacted at 80° C. with acetylene. 3-(Trimethylsilyl)propyl vinyl ether was obtained in 96% yield.