HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetylene → 3-(Trimethylsilyl)propyl vinyl ether
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetylene | HCID 6326 | — |
| Reactant | Potassium Hydroxide | HCID 14797 | — |
| Reactant | 1-Propanol, 3-(trimethylsilyl)- | HCID 76213 | — |
| Solvent | Dimethyl Sulfoxide | HCID 679 | — |
| Product | 3-(Trimethylsilyl)propyl vinyl ether | HCID 23363376 | 96% |
Reaction Steps
In a similar manner to Example 1, 25 g (0.19 mol) of 3-(trimethylsilyl)propanol, 2.5 g of KOH and 25 g of DMSO were reacted at 80° C. with acetylene. 3-(Trimethylsilyl)propyl vinyl ether was obtained in 96% yield.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05587503 |
| Source dataset | uspto-grants-1996_12 |
| ORD ID | ord-59e4293c63a04c8a88a6664dad1f4d7a |
| Source note | uspto-grants-1996_12 |