Methyl Acrylate → HCID 88359143, compound

Participants

Reaction Steps

To 4 moles of methyl acrylate were added 8.8 moles of dimethylaminopropylamine and the mixture was subjected to an addition reaction in the same manner as in Comparative Example 2. Then sodium methoxide was added thereto to conduct the amidation reaction. After completion of the reaction, the low-boiling-point substances were removed by distillation to give a crude N-dimethylaminopropyl-beta-dimethylaminopropylaminopropionamide. This contained about 13% of high-boiling-point impurities.

Provenance & Evidence