HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl chloroacetate → HCID 13336496, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl chloroacetate | HCID 7295 | — |
| Reactant | Azane;hydrate | HCID 12896473 | — |
| Reactant | HCID 67926483 | HCID 67926483 | — |
| Product | HCID 13336496 | HCID 13336496 | — |
Reaction Steps
According to the Procedure B of Example 1, the intermediate of the Example 3 was reacted with methyl chloroacetate. The resulting product methyl 4-(2ethyl-benzofuroyl)phenoxyacetate (Compound 11) was treated with concentrated ammonia water (28%) 100 ml and was stirred under ice-cooled condition for three hours. The white powder thus obtained, after drying was recrystallized from methanol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05004750 |
| Source dataset | uspto-grants-1991_04 |
| ORD ID | ord-1da61f8d497e41688548bf2f2ecbabed |
| Source note | uspto-grants-1991_04 |