反应详情

To a solution of 2-methyl-5-phenylpyridine (step 1) (169 mg) and N-bromosuccinimide (177 mg) in CCl4 (3 cc) was added benzoyl peroxide (25 mg) and the mixture irradiated with visible light for 5 hours under reflux. After removal of the solvent the residue was purified by chromatography to afford the title compound.

1. customthe mixture irradiated with visible light for 5 hours
2. temperatureunder reflux
3. customAfter removal of the solvent the residue
4. customwas purified by chromatography